Methyl Isocyanate → HCID 86737574, compound

HRID 127226Notes

Reaction equation

HRID 127226 reaction equation
[N:1](=[C:3]1[N:7]=[C:6]([CH2:8][CH2:9][CH2:10][CH3:11])[C:5]([CH3:13])([CH3:12])[S:4]1)[OH:2].[CH3:14][N:15]=[C:16]=[O:17]>>[CH3:14][NH:15][C:16]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH2:8][CH2:9][CH2:10][CH3:11])[C:5]([CH3:12])([CH3:13])[S:4]1)=[O:17]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 86737575HCID 86737575, compound

Product 1

HCID 86737574HCID 86737574, compound

Procedure

2-oxo-4-butyl-5,5-dimethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-butyl-5,5-dimethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 128°-130° C. The 2-oxo-4-butyl-5,5-dimethyl-3-thiazoline-oxime starting material melts at 117°-119° C.

Sources & evidence

ORD record
ord-3c24f81e75ae469eab8b22507a0bf0a9
Source dataset
uspto-grants-1981_03
Patent number
US04255436

Reaction notes

Loading…