Methyl Isocyanate → HCID 86737576, compound

HRID 127227Notes

Reaction equation

HRID 127227 reaction equation
[N:1](=[C:3]1[N:7]=[C:6]([CH3:8])[C:5]([CH3:13])([CH2:9][CH:10]([CH3:12])[CH3:11])[S:4]1)[OH:2].[CH3:14][N:15]=[C:16]=[O:17]>>[CH3:14][NH:15][C:16]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH3:8])[C:5]([CH3:13])([CH2:9][CH:10]([CH3:11])[CH3:12])[S:4]1)=[O:17]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 86737577HCID 86737577, compound

Product 1

HCID 86737576HCID 86737576, compound

Procedure

2-oxo-4,5-dimethyl-5-isobutyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4,5-dimethyl-5-isobutyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 99°-101° C. The 2-oxo-4,5-dimethyl-5-isobuty-3-thiazoline-oxime starting material melts at 105°-107° C.

Sources & evidence

ORD record
ord-03b8e97c925d44ee892b25ab87c649b1
Source dataset
uspto-grants-1981_03
Patent number
US04255436

Reaction notes

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