Methyl Isocyanate → HCID 86737578, compound

HRID 127228Notes

Reaction equation

[N:1](=[C:3]1[N:7]=[C:6]([CH3:8])[C:5]([CH3:14])([CH2:9][CH2:10][CH2:11][CH2:12][CH3:13])[S:4]1)[OH:2].[CH3:15][N:16]=[C:17]=[O:18]>>[CH3:15][NH:16][C:17]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH3:8])[C:5]([CH3:14])([CH2:9][CH2:10][CH2:11][CH2:12][CH3:13])[S:4]1)=[O:18]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 86737579HCID 86737579, compound

Product 1

HCID 86737578HCID 86737578, compound

Procedure

2-oxo-4,5-dimethyl-5-pentyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4,5-dimethyl-5-pentyl-3-thiazoline-O-(methylcarbamoyl)-oxime as a viscous oil; nD44.5 =1.5256. The 2-oxo-4,5-dimethyl-5-pentyl-3-thiazoline-oxime starting material melts at 104°-106° C.

Sources & evidence

ORD record: ord-9dfc5f3c48ef47ae8b962ab457610e84
Source dataset: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04255436

Reaction notes

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