HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22935623, compound → HCID 23113954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22935623 | HCID 22935623 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 23113954 | HCID 23113954 | 97% |
Reaction Steps
Using methyl 2-(3-bromo-2,4,5-trimethylphenoxy)isobutyrate obtained in Reference Example 22, the title compound was synthesized in the same manner as in Reference Example 15. Yield 97%. mp. 151–153° C. (hexane). 1H-NMR (CDCl3) δ: 1.59 (6H, s), 2.26 (3H, s), 2.33 (6H, s), 6.67 (1H, s), 9.60 (1H, br s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208495B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-c2ef42295ef74daaa29b66506bd25355 |
| Source note | uspto-grants-2007_04 |