HRID1272312

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：COc1ccc(N2CCN(c3c(C)c(C)c4c(c3C)C(O)(c3ccc(Cl)cc3)C(C)(C)O4)CC2)cc1

HCID58847327

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(N2CCN(c3c(C)c(C)c4c(c3C)C(c3ccc(Cl)cc3)C(C)(C)O4)CC2)cc1

HCID18456021

未命名化合物

收率 62%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Using 3-(4-chlorophenyl)-5-(4-(4-methoxyphenyl)piperazin-1-yl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-3-ol obtained in Example 62, the title compound was synthesized in the same manner as in Example 46. Yield 62%. mp. 181–183° C. (ethanol).