11-((Tert-butoxycarbonyl)amino)undecyl methanesulfonate → HCID 58803871, compound

HRID 1272394Notes

Reaction equation

HRID 1272394 reaction equation
[C:1]([O:5][C:6](=[O:29])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][O:19][CH2:20][CH2:21][O:22][CH2:23][CH2:24][O:25][CH2:26][CH2:27][OH:28])([CH3:4])([CH3:3])[CH3:2].C(OC(NCCCCCCCCCCC[O:49][S:50]([CH3:53])(=O)=[O:51])=O)(C)(C)C>>[C:1]([O:5][C:6]([NH:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][O:19][CH2:20][CH2:21][O:22][CH2:23][CH2:24][O:25][CH2:26][CH2:27][O:28][S:50]([CH3:53])(=[O:51])=[O:49])=[O:29])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 5880386211-((Tert-butoxycarbonyl)amino)undecyl methanesulfonateHCID 58803864HCID 58803864, compound

Product 1

HCID 58803871HCID 58803871, compound

Procedure

Compound 16 was prepared from compound 4 using methods analogous to the preparation of compound 3 (Example 1, step C). 1H NMR (DMSO-d6) δ 6.95 (t, 1H, J=5.5 Hz), 4.50 (m, 2H), 3.86 (m, 2H), 3.75–3.62 (m, 8H), 3.57 (t, 2H, J=7.2 Hz), 3.37 (s, 3H), 3.07 (q, 2H, J=6.0 Hz), 1.70–1.58 (m, 27H).

Sources & evidence

ORD record
ord-dbb976f795f548fbb602f1072f174aaf
Source dataset
uspto-grants-2007_04
Patent number
US07208322B2

Reaction notes

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