HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetic Acid → N-[2-(1H-Indol-2-yl)phenyl]-2-phenylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetic Acid | HCID 999 | — |
| Reactant | 2-(2-Aminophenyl)indole | HCID 735966 | — |
| Product | N-[2-(1H-Indol-2-yl)phenyl]-2-phenylacetamide | HCID 18455775 | 62% |
Reaction Steps
Prepared from 2-(2-aminophenyl) indole and phenylacetic acid in 62% yield following procedure 1. The product was crystallized from methanol. 100% Purity by LC/MS (230 DAD), Mass-spec [M+H+]=327, 1H NMR (MeOH-d4): 3.69 s (2H), 6.21 s (1H), 7.03 t, 7 Hz (1H), 7.12 t, 8 Hz (1H), 7.21–7.28 m (6H), 7.33–7.36 m (2H), 7.46 d, 8 Hz (1H), 7.54 dd, 7.1 Hz (1H), 7.89 d, 8 Hz (1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208493B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-8bcf5550b5224ff1a9c11b45601fa3fa |
| Source note | uspto-grants-2007_04 |