HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyphenylacetic acid → HCID 18455774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyphenylacetic acid | HCID 7134 | — |
| Reactant | 2-(2-Aminophenyl)indole | HCID 735966 | — |
| Product | HCID 18455774 | HCID 18455774 | 53% |
Reaction Steps
Prepared from 2-(2-aminophenyl) indole and 2-methoxyphenylacetic acid in 53% yield following procedure 1. The product was crystallized from acetonitrile. 100% Purity by LC/MS (230 DAD), Mass-spec [M+H+]=357, 1H NMR (MeOH-d4): 3.45 s (3H, OMe), 3.67 s (2H), 6.17 s (1H), 6.75 d, 8 Hz (1H), 6.83 t, 8 Hz (1H), 7.06 t, 8 Hz (1H), 7.14 t, 8 Hz (1H), 7.17–7.21 m (3H), 7.23–7.36 m (2H), 7.49 t, 8 Hz (2H), 8.13 d, 8 Hz (1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208493B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-41a22606bdde49c7a7daf9888a12197f |
| Source note | uspto-grants-2007_04 |