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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 127361Erstellt: 25. Oktober 2026

Benzenamine, 4-ethoxy-N-phenyl- → 6-(Dimethylamino)-3-[4-(ethylbenzylamino)phenyl]-3-[(4-ethoxyphenyl)phenylamino]phthalide

https://huagongshe.com/reaction/127361

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzenamine, 4-ethoxy-N-phenyl-HCID 70555—
Edukt5-(Dimethylamino)-2-[4-(ethylbenzylamino)benzoyl]benzoic acidHCID 20287186—
Produkt6-(Dimethylamino)-3-[4-(ethylbenzylamino)phenyl]-3-[(4-ethoxyphenyl)phenylamino]phthalideHCID 2028721350,5%

Reaktionsschritte

Following a procedure similar to that described in Example 4 but employing 4.0 g of 5-(dimethylamino)-2-[4-(ethylbenzylamino)benzoyl]benzoic acid and 2.2 g of 4-ethoxy-N-phenyl aniline there was obtained 3.0 g of 6-(dimethylamino)-3-[4-(ethylbenzylamino)phenyl]-3-[(4-ethoxyphenyl)phenylamino]phthalide, m.p. 148°-152° C. A toluene solution of the product contacted with acidic clay or phenolic resin developed an orange-colored image which changed to green on clay after fluorescent light exposure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04255577
Quelldatensatzuspto-grants-1981_03
ORD IDord-53685a230f574578bc3b154ae466d583
Quellennotizuspto-grants-1981_03