HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzenamine, 4-ethoxy-N-phenyl- → 6-(Dimethylamino)-3-[4-(ethylbenzylamino)phenyl]-3-[(4-ethoxyphenyl)phenylamino]phthalide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzenamine, 4-ethoxy-N-phenyl- | HCID 70555 | — |
| Edukt | 5-(Dimethylamino)-2-[4-(ethylbenzylamino)benzoyl]benzoic acid | HCID 20287186 | — |
| Produkt | 6-(Dimethylamino)-3-[4-(ethylbenzylamino)phenyl]-3-[(4-ethoxyphenyl)phenylamino]phthalide | HCID 20287213 | 50,5% |
Reaktionsschritte
Following a procedure similar to that described in Example 4 but employing 4.0 g of 5-(dimethylamino)-2-[4-(ethylbenzylamino)benzoyl]benzoic acid and 2.2 g of 4-ethoxy-N-phenyl aniline there was obtained 3.0 g of 6-(dimethylamino)-3-[4-(ethylbenzylamino)phenyl]-3-[(4-ethoxyphenyl)phenylamino]phthalide, m.p. 148°-152° C. A toluene solution of the product contacted with acidic clay or phenolic resin developed an orange-colored image which changed to green on clay after fluorescent light exposure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04255577 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-53685a230f574578bc3b154ae466d583 |
| Quellennotiz | uspto-grants-1981_03 |