HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 73866048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Phthalaldehydic acid | HCID 8406 | — |
| Reactant | HCID 12213306 | HCID 12213306 | — |
| Catalyst | Perchloric Acid | HCID 24247 | — |
| Product | HCID 73866048 | HCID 73866048 | — |
Reaction Steps
A mixture solution of the compound b (4.3 g), carboxybenzaldehyde (2 g), 70% perchloric acid (one drop), and acetic acid (10 ml) was refluxed for one hour. The precipitant was collected and recrystallized with a mixture solvent of ethanol and ether to obtain 4-(4-carboxystyryl)-2,6-diphenylpyrylium perchlorate (compound d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06156506 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-3eca412535dd40ad9a98464cb529782c |
| Source note | uspto-grants-2000_12 |