Hydrochloric Acid → 2,5-Dichloroaniline--hydrogen chloride (1/1)

Participants

Reaction Conditions

Reaction Steps

To a solution of 2,5-dichloroaniline (Aldrich, 1.5 g, 9 mmol) in methanol (10 mL) was added methanolic HCl (1M, 30 mL) at 4° C., then the reaction mixture was stirred at 25° C. for 30 minutes. The resulting solution was then evaporated and dried under vacuum to afford 1.6 g of 2,5-dichloroaniline hydrochloride (88% yield).

Provenance & Evidence