HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22120167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 22120165 | HCID 22120165 | — |
| Product | HCID 22120167 | HCID 22120167 | 88% |
Reaction Steps
Utilizing a procedure analogous to that of Example 16(b), 671 mg (1.7 mmol) of 6-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyloxy)naphthoyl chloride were reacted with 10 ml of aqueous ammonia (32%) to provide 560 mg (88%) of the expected amide, having a melting point of 175°-6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06156750 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-d0bb503b258b485baa121977d8369152 |
| Source note | uspto-grants-2000_12 |