HCID 22120851, compound → HCID 22120772, compound

HRID 1274233Notes

Reaction equation

HRID 1274233 reaction equation
C([O:3][C:4](=[O:37])[CH:5]([C:23]1[S:24][C:25]([CH2:28][C:29]2[CH:34]=[CH:33][C:32]([O:35][CH3:36])=[CH:31][CH:30]=2)=[CH:26][CH:27]=1)[NH:6][C:7](=[O:22])[CH:8]([CH2:17][S:18]C(=O)C)[CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)C>C(Cl)(Cl)Cl>[CH3:36][O:35][C:32]1[CH:31]=[CH:30][C:29]([CH2:28][C:25]2[S:24][C:23]([CH:5]([C:4]([OH:37])=[O:3])[NH:6][C:7](=[O:22])[CH:8]([CH2:17][SH:18])[CH2:9][CH2:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=3)=[CH:27][CH:26]=2)=[CH:34][CH:33]=1

Participants

3

Reactant 1

HCID 22120851HCID 22120851, compound

Product 1

HCID 22120772HCID 22120772, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

The title compound was prepared from 2-[5-(4-methoxybenzyl)thien-2-yl]-N-[2-(acetylthiomethyl)-4-phenylbutyryl]glycine ethyl ester (Description 66) by the procedure described in Example 24. vmax (CHCl3) 3423, 1724 and 1674 cm-1. m/z 469 (M+).

Sources & evidence

ORD record
ord-ff1d5eee18e8421cae84aa22744a2eb0
Source dataset
uspto-grants-2000_12
Patent number
US06156774

Reaction notes

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