Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isophthalic Acid | HCID 8496 | — |
| Reactant | 1,3-Benzenedimethanamine | HCID 15133 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131722195 | HCID 131722195 | 94.7% |
Reaction Steps
480 g of m-xylylenediamine (MXDA) and 580 g of isophthalic acid (IPA) were mixed with 1.0 kg of water and stirred at 90° C. for 1 hour. After becoming clear, the mixture solution was cooled to 25° C. The precipitate was then isolated by decantation, and vacuum dried at 25° C. for 24hours. 1.0 kg of MXDA/IPA salt was thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06156838 |
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| Source dataset | uspto-grants-2000_12 |
|---|
| ORD ID | ord-8f0fee510ec84c808c9678ef51b8fc93 |
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| Source note | uspto-grants-2000_12 |
|---|
