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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1274465Generated: October 31, 2026

Allyl bromide → Allyl 3,5-dimethylphenyl ether

https://huagongshe.com/reaction/1274465

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl bromideHCID 7841—
Reactant3,5-DimethylphenolHCID 7948—
ReactantPotassium CarbonateHCID 11430—
SolventAcetoneHCID 180—
ProductAllyl 3,5-dimethylphenyl etherHCID 257959100%

Reaction Steps

3,5-Dimethylphenol, 12.2 g (100 mmole), 10.8 ml (125 mmole) of allyl bromide, and 16.56 g (120 mmole) of potassium carbonate was dissolved and then refluxed in 50 ml acetone, with stirring, under nitrogen for 18 hours. The reaction was cooled, the insoluble inorganics were filtered off and stripped to give 16.2 g (100%) of subtitled product, which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06156748
Source datasetuspto-grants-2000_12
ORD IDord-f0257a6d43fc47c0adfb37c23782c151
Source noteuspto-grants-2000_12