Acetone → HCID 15483982, compound

HRID 1274813Notes

Reaction equation

HRID 1274813 reaction equation
[CH3:1][C:2]([CH3:4])=O.[CH3:5][O:6][C:7]1[CH:12]=[C:11]([O:13][C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([C:20]([F:23])([F:22])[F:21])[CH:15]=2)[N:10]=[C:9]([C:24]([NH:26][NH2:27])=[O:25])[CH:8]=1>>[C:2](=[N:27][NH:26][C:24](=[O:25])[C:9]1[CH:8]=[C:7]([O:6][CH3:5])[CH:12]=[C:11]([O:13][C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([C:20]([F:21])([F:22])[F:23])[CH:15]=2)[N:10]=1)([CH3:4])[CH3:1]

Participants

3

Reactant 2

HCID 180AcetoneHCID 70268884HCID 70268884, compound

Product 1

HCID 15483982HCID 15483982, compound

Procedure

Acetone (10 ml, 0.0015×91 mol) was added to 4-methoxy-6-[3-(trifluoromethyl)phenoxy] picolinic acid hydrazide (0.5 g, 0.0015 mol). The resultant mixture was stirred at room temperature for about one hours. The obtained reaction solution was concentrated, thereby obtaining an aimed product.

Workup

  1. customThe obtained reaction solution
  2. concentrationwas concentrated

Sources & evidence

ORD record
ord-f93a235f5db044589a70b5a88179b339
Source dataset
uspto-grants-2000_12
Patent number
US06159901

Reaction notes

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