Cyclopentanone → HCID 15483991, compound

HRID 1274821Notes

Reaction equation

HRID 1274821 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([C:16]([F:19])([F:18])[F:17])[CH:11]=2)[N:6]=[C:5]([C:20]([NH:22][NH2:23])=[O:21])[CH:4]=1.[C:24]1(=O)[CH2:28][CH2:27][CH2:26][CH2:25]1>C(OCC)C>[C:24]1(=[N:23][NH:22][C:20](=[O:21])[C:5]2[CH:4]=[C:3]([O:2][CH3:1])[CH:8]=[C:7]([O:9][C:10]3[CH:15]=[CH:14][CH:13]=[C:12]([C:16]([F:17])([F:18])[F:19])[CH:11]=3)[N:6]=2)[CH2:28][CH2:27][CH2:26][CH2:25]1

Participants

4

Reactant 2

HCID 8452CyclopentanoneHCID 70268884HCID 70268884, compound

Product 1

HCID 15483991HCID 15483991, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

4-methoxy-6-[3-(trifluoromethyl)phenoxy] picolinic acid hydrazide (0.40 g, 0.0012 mol) was mixed cyclopentanone (1.0 g, 0.0012×10 mol) and then with diethyl ether (about 10 ml). The resultant mixture was stirred at room temperature for about one hour. The obtained reaction solution was concentrated, thereby obtaining an aimed product.

Workup

  1. customThe obtained reaction solution
  2. concentrationwas concentrated

Sources & evidence

ORD record
ord-8f915f21242f42d3b1473a195c070a1a
Source dataset
uspto-grants-2000_12
Patent number
US06159901

Reaction notes

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