Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1274840Generated: October 31, 2026

Ethanolamine → HCID 22464717, compound

https://huagongshe.com/reaction/1274840

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolamineHCID 700—
ReactantEthanolHCID 702—
ReactantHCID 69959475HCID 69959475—
ProductHCID 22464717HCID 2246471793%

Reaction Steps

8.0 ml (133 mM [sic]) of ethanolamine were added to 35.6 g (114 mM [sic]) of 2-ethoxymethyleneamino-3-carboethoxy-5-methyl-5-dimethylcarbamoylthiophene [sic] in 200 ml of ethanol and refluxed for 2 h. The mixture was then concentrated under reduced pressure. 29.9 g (93%) of dark viscous oil were isolated.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06159962
Source datasetuspto-grants-2000_12
ORD IDord-1cfc1d89aa3d481eabb5658a4c50c55a
Source noteuspto-grants-2000_12