Sodium Hydroxide → HCID 70119419, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of N-phenoxycarbonyl-L-Valine (5.00 g, 21.1 mmol) in 350 mL of toluene cooled to 0° C. in an ice bath was added dropwise a solution of sodium hydroxide (840 mg, 21 mmol) in 2 mL of distilled water. The reaction was stirred at 0° C. for 2 hours and then concentrated under reduced pressure. The residue was chased three time with toluene (150 mL) to afford the title compound as an oil (6.03 g).

Provenance & Evidence