2-Propylphenol → HCID 22117438, compound

HRID 1275623Notes

Reaction equation

HRID 1275623 reaction equation
[CH2:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])[CH2:2][CH3:3].Cl[C:12]([CH3:20])([CH2:14][CH2:15][C:16](Cl)([CH3:18])[CH3:17])[CH3:13]>>[CH2:1]([C:4]1[C:5]([OH:10])=[CH:6][C:7]2[C:12]([CH3:20])([CH3:13])[CH2:14][CH2:15][C:16]([CH3:18])([CH3:17])[C:8]=2[CH:9]=1)[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 125702-PropylphenolHCID 80360Hexane, 2,5-dichloro-2,5-dimethyl-

Product 1

HCID 22117438HCID 22117438, compound

Procedure

In a manner similar to Example 7(a), by the reaction of 13.6 g (0.1 mol) of 2-n-propylphenol with 18.3 g (0.1 mol) of 2,5-dichloro-2,5-dimethylhexane, 11.6 g (65%) of the expected phenolic derivative of melting point 96-7° C. were obtained after chromatography on a silica column eluted with dichloromethane.

Workup

  1. customwere obtained after chromatography on a silica column
  2. washeluted with dichloromethane

Sources & evidence

ORD record
ord-9beafc60657d4a1fac88da76603c922b
Source dataset
uspto-grants-2000_12
Patent number
US06162815

Reaction notes

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