HCID 9930103, compound → HCID 22480383, compound

HRID 1275708Notes

Reaction equation

HRID 1275708 reaction equation
[Cl:1][C:2]1[S:6][C:5]([CH2:7][N:8]2[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[C:10]([C:17]3[O:18][C:19]([C:22](OCC)=[O:23])=[CH:20][CH:21]=3)=[N:9]2)=[CH:4][CH:3]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Cl:1][C:2]1[S:6][C:5]([CH2:7][N:8]2[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[C:10]([C:17]3[O:18][C:19]([CH2:22][OH:23])=[CH:20][CH:21]=3)=[N:9]2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 9930103HCID 9930103, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 22480383HCID 22480383, compound

Procedure

The compound was prepared similarly to Example 14 from 1-((5-chloro-2-thienyl)methyl)-3-(5-ethoxycarbonyl-2-furyl)indazole by reduction with lithium aluminum hydride.

Sources & evidence

ORD record
ord-f48b20add6a94d11b2f15b1039f3d2a1
Source dataset
uspto-grants-2000_12
Patent number
US06162819

Reaction notes

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