HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5,5-dimethyl-2-cyclohexen-1-one → HCID 22117841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5,5-dimethyl-2-cyclohexen-1-one | HCID 136680 | — |
| Reactant | HCID 22117852 | HCID 22117852 | — |
| Product | HCID 22117841 | HCID 22117841 | — |
Reaction Steps
Reaction of 3-amino-5,5-dimethyl-2-cyclohexen-1-one with 4-nitro-3-benzyloxybenzaldehyde dimethyl acetal in an analogous manner to that described in Example 1, gave 9-(3-benzyloxy-4-nitrophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from methanol/water gave a yellow crystalline solid of melting point 239-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162918 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-a8c8448f2f3f45f1bc98337dc11a32f3 |
| Source note | uspto-grants-2000_12 |