HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromobenzaldehyde → HCID 14573955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromobenzaldehyde | HCID 81129 | — |
| Reactant | 3-Amino-5,5-dimethyl-2-cyclohexen-1-one | HCID 136680 | — |
| Product | HCID 14573955 | HCID 14573955 | — |
Reaction Steps
3-Amino-5,5-dimethyl-2-cyclohexen-1-one was reacted with 2-bromobenzaldehyde in an analogous manner to that described in Example 1 to give 9-(2-bromophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from dimethylformamide/water gave a yellow powder of melting point >285° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162918 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-af58a5b331e74992ace9da76f4a1af5d |
| Source note | uspto-grants-2000_12 |