HRID1275882
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The subtitle compound was prepared from the product of example 1 step (iii) (1.0 g) and 2-(bromomethyl)-5-thiazolecarboxylic acid ethyl ester (0.9 g) according to the method of example 1 step (iv). The reaction mixture was evaporated to dryness under reduced pressure and the crude product was recrystallised from ethyl acetate/methanol. Yield 0.78 g.
WORKUP
后处理
- customThe reaction mixture was evaporated to dryness under reduced pressure
- customthe crude product was recrystallised from ethyl acetate/methanol