HRID1275882

反应详情

EQUATION

反应方程式

HRID 1275882 的结构方程式

PROCEDURE

实验过程

The subtitle compound was prepared from the product of example 1 step (iii) (1.0 g) and 2-(bromomethyl)-5-thiazolecarboxylic acid ethyl ester (0.9 g) according to the method of example 1 step (iv). The reaction mixture was evaporated to dryness under reduced pressure and the crude product was recrystallised from ethyl acetate/methanol. Yield 0.78 g.

WORKUP

后处理

  1. customThe reaction mixture was evaporated to dryness under reduced pressure
  2. customthe crude product was recrystallised from ethyl acetate/methanol