HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromobenzyl bromide → 2-[2-[2-[3-Bromophenyl]ethyl]phenyl]-4,5-dihydro-4,4-dimethyloxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromobenzyl bromide | HCID 69979 | — |
| Reactant | 4,4-Dimethyl-2-(2-methylphenyl)-4,5-dihydro-1,3-oxazole | HCID 10487889 | — |
| Product | 2-[2-[2-[3-Bromophenyl]ethyl]phenyl]-4,5-dihydro-4,4-dimethyloxazole | HCID 22117263 | — |
Reaction Steps
The subtitle compound was prepared from the product of step (i) (1 g) and 3-bromobenzylbromide (1.32 g) according to the method of example 21 step (ii). Purification was by chromatography eluting with 5-10% ethyl acetate inisohexane. Yield 0.64 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162808 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-6ba459a5da5d465f8b78a963cdf4d369 |
| Source note | uspto-grants-2000_12 |