反应详情

The subtitle compound was prepared from 5-bromo-2,4-bis(1,1-dimethylethoxy)pyrimidine (example step(i)) (3.5 g) and 10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-one (2.41 g) according to the method of example 1 step (iii). Purification was by chromatography eluting with 2% ethanol in dichloromethane. Yield 2.17 g. Used directly in the next step.

1. customPurification
2. washeluting with 2% ethanol in dichloromethane