HCID 22117206, compound → HCID 178435471, compound

HRID 1275921Notes

Reaction equation

HRID 1275921 reaction equation
[CH2:1]([C:3]1[CH:35]=[CH:34][C:6]2[CH:7]([C:17]3[C:18](=[S:33])[NH:19][C:20](=[O:32])[N:21]([CH2:23][C:24]4[O:28][C:27]([C:29]([OH:31])=O)=[CH:26][CH:25]=4)[CH:22]=3)[C:8]3[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][C:9]=3[CH:10]=[CH:11][C:5]=2[CH:4]=1)[CH3:2].[NH2:36][C:37]1[NH:41][N:40]=[N:39][N:38]=1>>[CH2:1]([C:3]1[CH:35]=[CH:34][C:6]2[CH:7]([C:17]3[C:18](=[S:33])[NH:19][C:20](=[O:32])[N:21]([CH2:23][C:24]4[O:28][C:27]([C:29]([NH:36][C:37]5[NH:41][N:40]=[N:39][N:38]=5)=[O:31])=[CH:26][CH:25]=4)[CH:22]=3)[C:8]3[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][C:9]=3[CH:10]=[CH:11][C:5]=2[CH:4]=1)[CH3:2]

Participants

3

Reactant 2

HCID 22117206HCID 22117206, compoundHCID 178509299HCID 178509299, compound

Product 1

HCID 178435471HCID 178435471, compound

Procedure

The title compound was prepared from the product of example 31(0.93 g) and amino tetrazole (0.3 g) according to the method of example 10 step (i). Purification was by precipitation from ethyl acetate-iso-hexane. Yield 0.426 g.

Workup

  1. customPurification
  2. customwas by precipitation from ethyl acetate-iso-hexane

Sources & evidence

ORD record
ord-fdc33e261d7f42ba8572a0fb6afb9cd3
Source dataset
uspto-grants-2000_12
Patent number
US06162808

Reaction notes

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