HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 15886605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Enrasentan | HCID 178103 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 15886605 | HCID 15886605 | — |
Reaction Steps
This intermediate was isolated by flash column chromatography (SiO2, EtOAc/Hexane=30/70) of a sample of the crude reaction mixture from the preparation of (1S, 2R, 3S)-3-[2-(2-Hydroxyeth-1-yloxy)-4-methoxyphenyl)-1-(3,4-methylendioxyphenyl)-5-propoxyindane-2-carboxylic acid described above prior to the saponification with lithium hydroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06162932 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-1ca1b2eb138147c1a655f5e1ecc528f3 |
| Source note | uspto-grants-2000_12 |