HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Ethyl-2-methylpyridine → (5-Ethylpyridin-2-yl)methyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Ethyl-2-methylpyridine | HCID 7728 | — |
| Reactant | 2-Pyridinemethanol, 5-methyl-, 2-acetate | HCID 12325384 | — |
| Product | (5-Ethylpyridin-2-yl)methyl acetate | HCID 14346253 | 89% |
Reaction Steps
This synthesis was performed analogously to the synthesis reported for 2-acetoxymethyl-5-methyl pyridine. Starting from 5-ethyl-2-methyl pyridine (35.10 g, 290 mmol), pure 2-acetoxymethyl-5-ethyl pyridine (46.19 g, 258 mmol, 89%) was obtained as a slightly yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06165963 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-0f7ac4c339e347489d69a202ebdc9887 |
| Source note | uspto-grants-2000_12 |