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HRID1276084

反应详情

EQUATION

反应方程式

HRID 1276084 的结构方程式

REACTANTS

反应物

3
结构：BrCC1CO1
HCID18430

Epibromohydrin

C3H5BrO

结构：CC(C)n1c(=O)n(C)c2cc(-c3ncc(C(F)(F)F)cc3Cl)ccc21
HCID22114840

未命名化合物

结构：CC(C)n1c(=O)[nH]c2cc(-c3ncc(C(F)(F)F)cc3Cl)ccc21
HCID22114855

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)n1c(=O)n(CC2CO2)c2cc(-c3ncc(C(F)(F)F)cc3Cl)ccc21
HCID22114866

未命名化合物

收率 83%

PROCEDURE

实验过程

In a similar manner to the preparation of 5-(3-chloro-5-trifluoromethylpyridin-2-yl)-3-methyl-1-(1-methylethyl)benzimidazol-2-one described above, 2.5 g of 5-(3-chloro-5-trifluoromethyl-pyridin-2yl)-1-(1-methylethyl)benzimidazol-2-one and 1.0 g of epibromohydrin gave 2.4 g of colorless crystals. Yield: 83%; m.p.: 110-111° C.