2-(2-Chloroethoxy)tetrahydro-2H-pyran → HCID 22116122, compound

HRID 1276319Notes

Reaction equation

HRID 1276319 reaction equation
[CH2:1]([C:3]1([CH3:13])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[NH:5][C:4]1=[O:12])[CH3:2].Cl[CH2:15][CH2:16][O:17]C1CCCCO1>>[CH2:1]([C:3]1([CH3:13])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]([CH2:15][CH2:16][OH:17])[C:4]1=[O:12])[CH3:2]

Participants

3

Reactant 2

HCID 2549512-(2-Chloroethoxy)tetrahydro-2H-pyranHCID 14359628HCID 14359628, compound

Product 1

HCID 22116122HCID 22116122, compound

Procedure

Prepared from 3-ethyl-3-methylindol-2(3H)-one (prepared by the method of Endler and Becker; Organic Syntheses Coll. vol. 4 page 657) and 2-(2-chloroethoxy)tetrahydro-2H-pyran as described in above.

Workup

  1. customprepared by the method of Endler and Becker

Sources & evidence

ORD record
ord-3457691e6f8447f8bf2cd4e1e5c67729
Source dataset
uspto-grants-2000_12
Patent number
US06166040

Reaction notes

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