tert-Butyl bromoacetate → HCID 12135274, compound

Participants

Reaction Steps

This compound was prepared from (2-benzyl-benzofuran-3-yl)-(3,5-diiodo-4-hydroxy-phenyl)-methanone and tert-butyl bromoacetate in substantially the same manner, as described in Example 2. Formic acid was used in the place of trifluoroacetic acid. The product was obtained as an off-white solid, mp 144-146° C.; MS m/e 638 (M+); Analysis for: C24H16I2O5Calc'd: C, 45.17; H, 2.53 Found: C, 44.19; H, 2.42

Provenance & Evidence