HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 57153492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 57025299 | HCID 57025299 | — |
| Catalyst | Tetrabutylammonium hydrogen sulfate | HCID 94433 | — |
| Product | HCID 57153492 | HCID 57153492 | — |
Reaction Steps
8.0 g (26.6 mmol) of compound A that is presented according to Example 1c is mixed with 80 ml of a 50% potassium hydroxide solution, 32 ml of benzyl chloride and 1 g of tetrabutyl-ammonium hydrogen sulfate. It is allowed to react for about 4 hours at 50° C. while being stirred vigorously, and the crude mixture, which contains the title compound, is further reacted without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166075 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-68c9315e7f6b480da669d5524b128f22 |
| Source note | uspto-grants-2000_12 |