HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Bromide → 1-(Phenylmethyl)-1H-1,2,4-triazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Bromide | HCID 7498 | — |
| Edukt | 1H-1,2,4-Triazole | HCID 9257 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 1-(Phenylmethyl)-1H-1,2,4-triazole | HCID 22458 | — |
Reaktionsschritte
A mixture of 34.2 parts by weight of benzyl bromide, 13.8 parts by weight of 1,2,4-triazole and 41.4 parts by weight of potassium carbonate in 150 parts by weight of acetonitrile is refluxed for 10 hours while stirring. The mixture is filtered and the filtrate is evaporated to dryness and recrystallized from a mixture of toluene and cyclohexane. There is obtained 21 parts by weight of 1-benzyl-1,2,4-triazole; m.p.: 58° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04256754 |
| Quelldatensatz | uspto-grants-1981_03 |
| ORD ID | ord-26e929fcdfca4b17826444a9104df6a9 |
| Quellennotiz | uspto-grants-1981_03 |