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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 127660Erstellt: 25. Oktober 2026

Benzyl Bromide → 1-(Phenylmethyl)-1H-1,2,4-triazole

https://huagongshe.com/reaction/127660

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzyl BromideHCID 7498—
Edukt1H-1,2,4-TriazoleHCID 9257—
EduktPotassium CarbonateHCID 11430—
LösungsmittelAcetonitrileHCID 6342—
Produkt1-(Phenylmethyl)-1H-1,2,4-triazoleHCID 22458—

Reaktionsschritte

A mixture of 34.2 parts by weight of benzyl bromide, 13.8 parts by weight of 1,2,4-triazole and 41.4 parts by weight of potassium carbonate in 150 parts by weight of acetonitrile is refluxed for 10 hours while stirring. The mixture is filtered and the filtrate is evaporated to dryness and recrystallized from a mixture of toluene and cyclohexane. There is obtained 21 parts by weight of 1-benzyl-1,2,4-triazole; m.p.: 58° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04256754
Quelldatensatzuspto-grants-1981_03
ORD IDord-26e929fcdfca4b17826444a9104df6a9
Quellennotizuspto-grants-1981_03