HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenoxybenzaldehyde → (4-Phenoxyphenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenoxybenzaldehyde | HCID 66139 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | (4-Phenoxyphenyl)methanol | HCID 826195 | 96.6% |
Reaction Steps
Sodium borohydride (0.48 g) was added to a solution of 4.96 g of 4-phenoxybenzaldehyde in 20 ml of ethanol, and the mixture was stirred at room temperature for 1.5 hours. After the completion of the concentration, the residue was extracted with tert-butylmethyl ether and with water. The organic layer was concentrated to give 4.84 g of 4-phenoxybenzyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06166219 |
| Source dataset | uspto-grants-2000_12 |
| ORD ID | ord-b471ca45d4ad4837b0f507ed0287fefc |
| Source note | uspto-grants-2000_12 |