HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20285880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 13545960 | HCID 13545960 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 20285880 | HCID 20285880 | — |
Reaction Steps
52 parts of 8-nitro-naphthalene-1,4-dicarboxylic acid are dissolved in 700 parts of absolute ethyl alcohol and the solution is boiled under reflux for 12 hours whilst continuously passing in hydrogen chloride gas. The resulting solution is evaporated in vacuo. The 4-ethoxycarbonyl-8-nitro-naphthalene-1-carboxylic acid of the formula ##STR17## which is obtained in this way, melts at 178° to 180°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04256896 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-780931521a7449039a680dbce13e8f82 |
| Source note | uspto-grants-1981_03 |