HCID 23454104, compound → HCID 178433298, compound

HRID 1277444Notes

Reaction equation

HRID 1277444 reaction equation
[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2].N[CH2:20][CH2:21][S:22][CH2:23][N:24]1N=CC=N1>C(#N)C>[N+:1]([CH:4]=[C:5]([NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:23]1[S:22][CH:21]=[CH:20][N:24]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 23454104HCID 23454104, compoundHCID 178503826HCID 178503826, compound

Product 1

HCID 178433298HCID 178433298, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Reaction of 1-nitro-2-methylthio-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]ethylene with an excess of 2-[(2-aminoethyl)thiomethyl]triazole according to the procedure of Example 3, results in the production of 1-nitro-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]-2-[2-(2-thiazolylmethylthio)ethylamino]ethylene, m.p. 110°-120° (from acetonitrile).

Sources & evidence

ORD record
ord-b21ca0a7d463411896ade528ced1e053
Source dataset
uspto-grants-1981_07
Patent number
US04277485

Reaction notes

Loading…