2,3-Dihydroxybutanedioic Acid → HCID 23454153, compound

HRID 1277497Notes

Reaction equation

HRID 1277497 reaction equation
[NH2:1][CH2:2][C:3]([NH:5][C:6]([CH3:13])([CH3:12])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])=[O:4].[C:14]([OH:23])(=[O:22])[CH:15]([CH:17]([C:19]([OH:21])=[O:20])[OH:18])[OH:16]>CO>[C:19]([CH:17]([CH:15]([C:14]([OH:23])=[O:22])[OH:16])[OH:18])([OH:21])=[O:20].[NH2:1][CH2:2][C:3]([NH:5][C:6]([CH3:12])([CH3:13])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])=[O:4]

Participants

4

Reactant 2

HCID 8752,3-Dihydroxybutanedioic AcidHCID 128299A 643C

Product 1

HCID 23454153HCID 23454153, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

2-Amino-N-(1,1-dimethylhexyl)acetamide (5 g) was added to a solution of tartaric acid (4.03 g) in methanol (50 ml). The solution was concentrated to dryness on a rotary evaporator and yielded a white solid, m.p. 150.5° C.

Workup

  1. concentrationThe solution was concentrated to dryness on a rotary evaporator
  2. customyielded a white solid, m.p. 150.5° C.

Sources & evidence

ORD record
ord-3db168e1d8d14415b6f59e290692af5a
Source dataset
uspto-grants-1981_07
Patent number
US04277498

Reaction notes

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