反应详情

2-Amino-N-(1,1-dimethylhexyl)acetamide (5 g) was dissolved in ether (25 ml)and glacial acetic acid (1.61 g) added. Petroleum distillate (b.p. 40°-60° C.) was added whereupon an oil separated. The mixture was cooled and the resulting solid filtered off yielding 2-amino-N-(1,1-dimethylhexyl)acetamide acetate, m.p. 64° C.

1. customseparated
2. temperatureThe mixture was cooled
3. filtrationthe resulting solid filtered off