Acetic Acid → HCID 85934109, compound

HRID 1277498Notes

Reaction equation

HRID 1277498 reaction equation
[NH2:1][CH2:2][C:3]([NH:5][C:6]([CH3:13])([CH3:12])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])=[O:4].[C:14]([OH:17])(=[O:16])[CH3:15]>CCOCC>[C:14]([OH:17])(=[O:16])[CH3:15].[NH2:1][CH2:2][C:3]([NH:5][C:6]([CH3:12])([CH3:13])[CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])=[O:4]

Participants

4

Reactant 2

HCID 176Acetic AcidHCID 128299A 643C

Product 1

HCID 85934109HCID 85934109, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

2-Amino-N-(1,1-dimethylhexyl)acetamide (5 g) was dissolved in ether (25 ml)and glacial acetic acid (1.61 g) added. Petroleum distillate (b.p. 40°-60° C.) was added whereupon an oil separated. The mixture was cooled and the resulting solid filtered off yielding 2-amino-N-(1,1-dimethylhexyl)acetamide acetate, m.p. 64° C.

Workup

  1. customseparated
  2. temperatureThe mixture was cooled
  3. filtrationthe resulting solid filtered off

Sources & evidence

ORD record
ord-5dde2f53ee5940ac875109fb213b9df8
Source dataset
uspto-grants-1981_07
Patent number
US04277498

Reaction notes

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