HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73678918, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Reactant | HCID 54113944 | HCID 54113944 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 73678918 | HCID 73678918 | 200.5% |
Reaction Steps
The procedure described in Example (1b) is repeated, except that 113 g (0.41 mol) of 3,3-dimethyl-12-hexyl-1-aza-1,5,9-cyclododecatriene, 33 g (0.202 mol) of hydroxylamine sulfate, 50 g of concentrated hydrochloric acid and 250 ml of water are used. Working up yields 125 g (0.405 mol) of 2,2-dimethyl-11-n-hexyl-11-amino-undeca-4,8-dienal oxime; yield 99% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277621 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-79242778b62545ac9e0deeba0e26d836 |
| Source note | uspto-grants-1981_07 |