HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2,2-Dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal phenylhydrazone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | 3,3-Dimethyl-12-isopropyl-1-aza-1,5,9-cyclododecatriene | HCID 557512 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,2-Dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal phenylhydrazone | HCID 70506396 | 100% |
Reaction Steps
The procedure described in Example 1(b) is repeated, except that 23.3 g (0.1 mol) of 3,3-dimethyl-12-isopropyl-1-aza-1,5,9-cyclododecatriene, 20 gof 37% hydrochloric acid, 20 ml of water and 10.8 g (0.1 mol) of phenylhydrazine are used. Working up as described in Example 1(b) yields 34.1 g (0.1 mol) of 2,2-dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal phenylhydrazone; yield 100% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04277621 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-89f088b3859b4c36983e6ad7132e19f3 |
| Source note | uspto-grants-1981_07 |