HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12917674, compound → HCID 12917673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12917674 | HCID 12917674 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12917673 | HCID 12917673 | 96.6% |
Reaction Steps
α-Methylthio-α-(p-(o-carboxybenzoylamino)phenyl)propionic acid (146 mg) was dissolved in 1 ml of acetic acid, and the solution was heated under reflux for 3 hours. Acetic acid was removed under reduced pressure to afford 134 mg of α-methylthio-α-(p-phthalimidophenyl)propionic acid as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04278802 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-b0bb76d04b7b4360ae7c4b9603b5e425 |
| Source note | uspto-grants-1981_07 |