3,5-Dinitrobenzoyl chloride → HCID 12898841, compound

Participants

Reaction Steps

To 8.0 g. (0.05 mole) of 3-amino-1-cyclohexylpyrrolidine in chloroform was added with stirring 12 g. (0.052 mole) of 3,5-dinitrobenzoylchloride. After stirring one hour, the solution was extracted with dilute sodium hydroxide, dried over sodium sulfate and concentrated. The residue was recrystallized from isooctane-ethyl acetate. The product weighed 5.1 g. (29%) and melted at 159°-161° C.

Provenance & Evidence