HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 967209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 2-Iodobenzoyl chloride | HCID 69112 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 967209 | HCID 967209 | — |
Reaction Steps
A solution of 15 ml of benzylamine in 20 ml of tetrahydrofuran was reacted with a solution of 8.0 g of o-iodobenzoyl chloride in 20 ml of tetrahydrofuran in accordance with the procedure of Example 3. There was obtained by recrystallization from benzene 9.1 g of N-benzyl-o-iodobenzamide, m.p. 122°-123°, Rf 0.78.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279887 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-68fb223505b5424594055f26c1c2e670 |
| Source note | uspto-grants-1981_07 |