HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 70529163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | (R)-5,6,6a,7-Tetrahydro-1,2,9,10-tetramethoxy-6-methyl-4H-dibenzo(de,g)quinoline | HCID 1078819 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 70529163 | HCID 70529163 | — |
Reaction Steps
For making l-glaucine hydroiodide, a quantity of l-glaucine was dissolved in 2 n hydrochloric acid and the solution reacted with saturated potassium iodide solution. The resulting crystalline precipitate was recrystallized from a mixture of methyl alcohol and ether. This gave a crystalline, yellowish glaucine hydroiodide with a melting point of 238° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279914 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-89e3e405d3eb469cb54307c647dcde49 |
| Source note | uspto-grants-1981_07 |