3,4-Dichlorophenyl isocyanate → HCID 53701285, compound

HRID 1278013Notes

Reaction equation

HRID 1278013 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]=[C:10]=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8].[Cl:12][C:13]([Cl:17])=[CH:14][CH2:15][NH2:16]>C(OCC)C>[Cl:12][C:13]([Cl:17])=[CH:14][CH2:15][NH:16][C:10]([NH:9][C:4]1[CH:5]=[CH:6][C:7]([Cl:8])=[C:2]([Cl:1])[CH:3]=1)=[O:11]

Participants

4

Reactant 2

HCID 76073,4-Dichlorophenyl isocyanateHCID 234236383,3-Dichloroprop-2-en-1-amine

Product 1

HCID 53701285HCID 53701285, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To 0.02 mol of 3,4-dichlorophenylisocyanate, dissolved in 40 ml of ethyl ether, were admixed, at room temperature, 0.02 mol of N-(3,3-dichloroallyl)-amine (prepared starting from 3,3-trichloropropene with hexamethylentetramine--see e.g., Italian patent application No. 28,867 A/76).

Workup

  1. customwere admixed, at room temperature

Sources & evidence

ORD record
ord-c2b9a86d735949fcb49bd9a6f0be0c1f
Source dataset
uspto-grants-1981_07
Patent number
US04279927

Reaction notes

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