HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 70574986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chlorobenzyl cyanide | HCID 241582 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 70574986 | HCID 70574986 | — |
Reaction Steps
Stir 106 g of 2-methoxypyrroline-1, 243.5 g of 4-chlorobenzylcyanide and 9 ml of triethylamine for 20 hours at 110°. After cooling, add 200 ml of diethyl ether thereto and filter off the formed precipitate (80.9 of the title compound). Distil off the solvent and the 4-chlorobenzylcyanide under a vacuum to obtain a further 42 g of the title compound (m.p. 135° to 137°) for a total yield of 122.9 g (52% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279918 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-38e7ad428fbd4aff8095f5d1a140cffe |
| Source note | uspto-grants-1981_07 |