HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylene Glycol → HCID 23452573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylene Glycol | HCID 8172 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 23452544 | HCID 23452544 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23452573 | HCID 23452573 | — |
Reaction Steps
Heat 0.8 g of 2-(4-chlorobenzyl)-1-[3-(4-fluorobenzoyl)propyl]pyrrolidine to 170° for 2 hours with 1 ml of hydrazine hydrate, 0.5 g of potassium hydroxide and 5 ml of triglycol. After cooling the obtained reaction mixture to ambient temperature, add water and diethyl ether thereto. Dry the ethereal phase over sodium sulfate and distil off the solvent to obtain the title compound as brownish viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279918 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-672f2d856d034d33806068a9f473dd91 |
| Source note | uspto-grants-1981_07 |