HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-Naphthohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Naphthalenecarboxylic acid, methyl ester | HCID 120056 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Naphthohydrazide | HCID 72689 | 86% |
Reaction Steps
A mixture of 21.5 g (0.116 mol) of methyl α-naphthoate, 50 ml of 80% water containing hydrazine, and 30 ml of methanol was refluxed for 3 hours and then the reaction mixture obtained was cooled to form crystals, which were recovered and washed with water to provide 19.0 g (yield 86%) of α-naphthoic acid hydrazide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279982 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-065dc10df9694d45acaa6529a46b89f9 |
| Source note | uspto-grants-1981_07 |