HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexachloroacetone → N-alpha-naphthoyl-N'-trichloroacetylhydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexachloroacetone | HCID 8303 | — |
| Reactant | 1-Naphthohydrazide | HCID 72689 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-alpha-naphthoyl-N'-trichloroacetylhydrazine | HCID 23452724 | 88.2% |
Reaction Steps
To a mixture of 100 ml of acetonitrile and 14.6 g (0.055 mol) of hexachloroacetone was added 9.3 g of α-naphthoic acid hydrazide thus obtained and the resultant mixture was refluxed with stirring for 4 hours. The precipitates formed were recovered by filtration to provide 14.6 g (yield 88%) of N-α-naphthoyl-N'-trichloroacetylhydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04279982 |
| Source dataset | uspto-grants-1981_07 |
| ORD ID | ord-dfbeb1db28c1493cb7631e9785c63ea6 |
| Source note | uspto-grants-1981_07 |